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Assessment of damage in ceramics and ceramic matrix composites using ultrasonic techniques

机译:使用超声技术评估陶瓷和陶瓷基复合材料的损伤

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摘要

This paper addresses the application of ultrasonic sensing to damage assessment in ceramics and ceramic matrix composites. It focuses on damage caused by thermal shock or oxidation at elevated temperatures, which often results in elastic anisotropy. This damaged-induced anisotropy is determined by measuring the velocities of ultrasonic waves in different propagation directions. Thermal shock damage is assessed in ceramic samples of reaction bonded silicon nitride (RBSN). Thermal shock treatment from different temperatures up to 1000 C is applied to produce the microcracks. Results indicate that most microcracks produced by thermal shock are located near sample surfaces. Ultrasonic measurements using the surface wave method are found to correlate well with measurements of degradation of mechanical properties obtained independently by other authors using destructive methods. Oxidation damage is assessed in silicon carbide fiber/reaction bonded silicon nitride matrix (SCS-6/RBSN) composites. The oxidation is done by exposing the samples in a flowing oxygen environment at elevated temperatures, up to 1400 C, for 100 hr. The Youngs' modulus in the fiber direction as obtained from ultrasonic measurements decreases significantly at 600 C but retains its original value at temperatures above 1200 C. This agrees well with the results of destructive tests by other authors. On the other hand, the transverse moduli obtained from ultrasonic measurements decrease continually until 1200 C. Measurements on the shear stiffnesses show behavior similar to the transverse moduli. The results of this work show that the damage-induced anisotropy in both ceramics and ceramic matrix composites can be determined successfully by ultrasonic methods. This suggests the possibility of assessing damage severity using ultrasonic techniques.
机译:本文探讨了超声传感在陶瓷和陶瓷基复合材料损伤评估中的应用。它着重于高温下由热冲击或氧化引起的损坏,这通常会导致弹性各向异性。这种损坏引起的各向异性是通过测量超声波在不同传播方向上的速度来确定的。在反应结合氮化硅(RBSN)的陶瓷样品中评估了热冲击损伤。施加从高达1000°C的不同温度进行的热冲击处理,以产生微裂纹。结果表明,大多数由热冲击产生的微裂纹都位于样品表面附近。发现使用表面波方法进行的超声波测量与其他作者使用破坏性方法独立获得的机械性能下降的测量结果具有很好的相关性。在碳化硅纤维/反应结合的氮化硅基质(SCS-6 / RBSN)复合材料中评估了氧化损伤。氧化是通过将样品在不断流动的氧气环境中于1400°C的高温下暴露100小时来完成的。通过超声测量获得的纤维方向的杨氏模量在600°C时显着降低,但在1200°C以上的温度下保持其原始值。这与其他作者的破坏性测试结果十分吻合。另一方面,从超声测量获得的横向模量持续降低直至1200℃。抗剪刚度的测量显示出与横向模量相似的行为。这项工作的结果表明,通过超声方法可以成功地确定陶瓷和陶瓷基复合材料中的损伤诱导各向异性。这表明使用超声技术评估损害严重性的可能性。

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